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《滴答屋》贬顿中字在线观看-电影-德思影院

把男人当工具如鱼得水,把男人当靠山墙倒屋塌。

2024年12月21日,接下来的发现,是根据论文第57页中的这句话:

《滴答屋》贬顿中字在线观看-电影-德思影院

两年净利润下滑近99%

? 米特尔施泰特 (73')“为增加收入,我们和合作社展开合作,把龙柳枝进行深加工,变成一根根鲜艳漂亮的艺术品,或做成熏香条,广受客户喜欢。”薛立宪说。

《feirichangpaidui》yingshouguan yushuxinfuguzaoxingcanzaotucao2020-11-19 18:56·zhongguojilinwangjiemuxuanchuanjietuyouaiqiyichupin,yuzijiangheaiqiyixiaoguaishougongzuoshigongtongzhizuodechenjinshihudongtiaozhanzongyi《feirichangpaidui》dishierqishangjijijiangbochu,zuoweijiemudeshouguanzhizuo,THE9zaizheyiqizhongjitibianshengaozhongbiyesheng,yulidan、renjialun、xingfei、yuzuozuo、zhuzuowuwei“zishenbiyejianzhengren”yitongyinglailiaozhuanshudepaiduiwuhui。jiemuzhong,THE9shenchuanlifujingyanchuchang,yuwangqidehuoposatuoxiangbigengduoliaoyifenyouya,erwuwei“biyejianzhengren”zedanfuqiliaoweiTHE9chengyuanmendebiyezhengshugaizhangdezhongdan。weiliaonenggouxuandaozijixinyidechengyuan,jiabinmenjitidakainaodong,bieyangdeyouxiyaoqiushunjianjiqiTHE9chengyuandeshengfuyu,guochengzhongbujinyoulidanxianchangkuangpao“shitilangeng”,gengyourenjialunliyaozhaoxiaotangruduiquecanzaojujue。zhihoudequanxinyouxi“youyadedouji”tongyangyeshixiaoliaomanman,THE9chengyuangenjiabinzaiyicidapoguize,zhanxianfenzubattledeqiangjinshili,jiujingshishimeyangdebiaoxianlinglidanxianchangduiTHE9denvtuanshenfenbiaoshi“zhiyi”ne?lidandangchang“paolangeng”xuanren,zhaoxiaotangjujuerenjialunruduiyaoqingzuoweibenqijiemuzhongTHE9de“biyejianzhengren”,lidan、renjialun、xingfei、yuzuozuo、zhuzuowuweijiabinshouxianxuyaozuodebianshixuanchuzijixinyidechengyuanbingweiqigaozhongbiyezhengshugaizhang。weiliaonenggouxuandaozijixiangxuandechengyuan,jiweijiabinfenfenkaidongnaojin,gezhonghuashixuanrenbiaozhunlingTHE9xianchangkaishiliaoyichangyouguanyunqiyushilideqiangjinbattle。youxizhong,zuoweidiyigechuchanggaizhangdebiyejianzhengren,lidandangchangpaochu“shitilangeng”kaoyanTHE9chengyuandejiegengnengli,quebeitucaodaojutai“nian”。zhihourenjialungengshizaixuanzezhaoxiaotangjiaruzijiduiwushicanzaojujue,jiujingshishimeyangde“geng”lingxianchangzhongrenyanqianyiliang,zhaoxiaotangzuizhongyounengfouchenggongjiarurenjialundeduiwu?zhaoxiaotangyouxinenglizhejingdaizhongren,THE9beijiao“nvzisandatuanti”fenzujieshuhoubianyinglailiaobenqidiyigequanxinshengjideyouxi“youyadedouji”,zaizhegehuanjiezhong,meizuchengyuanduxuyaozaibeihoutieshangzihuoci,tongzuzhongdesuoyouzicikeyilianchengyijuhua,xianwanzhengkandaobingcaichuduishouzhengquejuzideduiwuhuodeshengli。youxikaishi,shenjingbaizhandeTHE9chengyuanbianyishuxizhizishunlidapoyouxiguize,kaishiliaoshiliqushengde“qiangzibaoweizhan”。qizhongzhaoxiaotangpingjieyijizhilichenggongyazhixiekeyin,shouhuliaozijiduiwudeshenmijuzi,shilizhiqiangredexianchangjinghu,namedaodishiruhedejiliebiaoxianshiTHE9denvtuanshenfenzaicizaodao“zhiyi”,youshishimelinglidanfachu“nvzisandatuanti”degantan?《feirichangpaidui》tebiebanbiyewuhuijikeshangxian,shuyupaiduidegushijijiangzanbie,danqingchunbusanchang,kuaileyongbutingxie!shizhijinri,50kuaiqianyijingtigaodaoliao200kuaiqian。

继(Ji)续(Xu)分(Fen)享(Xiang)一(Yi)一(Yi)waters 2695高(Gao)效(Xiao)液(Ye)相(Xiang)色(Se)谱(Pu)仪(Yi)SOP2020-09-13 20:49·搞(Gao)实(Shi)验(Yan)的(De)小(Xiao)李(Li)1.目(Mu)的(De):建(Jian)立(Li)本(Ben)公(Gong)司(Si)化(Hua)验(Yan)室(Shi)用(Yong)Waters e2695高(Gao)效(Xiao)液(Ye)相(Xiang)使(Shi)用(Yong)与(Yu)维(Wei)护(Hu)的(De)标(Biao)准(Zhun)操(Cao)作(Zuo)程(Cheng)序(Xu),规(Gui)范(Fan)Waters高(Gao)效(Xiao)液(Ye)相(Xiang)的(De)正(Zheng)确(Que)使(Shi)用(Yong)和(He)校(Xiao)准(Zhun),保(Bao)证(Zheng)测(Ce)量(Liang)结(Jie)果(Guo)正(Zheng)确(Que)无(Wu)误(Wu)。2.范(Fan)围(Wei):适(Shi)用(Yong)于(Yu)本(Ben)公(Gong)司(Si)化(Hua)验(Yan)室(Shi)Waters e2695高(Gao)效(Xiao)液(Ye)相(Xiang)的(De)操(Cao)作(Zuo)与(Yu)维(Wei)护(Hu)。3.术(Shu)语(Yu):4.职(Zhi)责(Ze):化(Hua)验(Yan)室(Shi)QC人(Ren)员(Yuan)负(Fu)责(Ze)本(Ben)规(Gui)程(Cheng)的(De)执(Zhi)行(Xing);质(Zhi)保(Bao)部(Bu)长(Chang)负(Fu)责(Ze)本(Ben)规(Gui)程(Cheng)执(Zhi)行(Xing)情(Qing)况(Kuang)的(De)监(Jian)督(Du)。5.操(Cao)作(Zuo)程(Cheng)序(Xu)与(Yu)方(Fang)法(Fa):5.1 仪(Yi)器(Qi)组(Zu)成(Cheng)及(Ji)电(Dian)源(Yuan):5.1.1 仪(Yi)器(Qi)组(Zu)成(Cheng):本(Ben)仪(Yi)器(Qi)由(You)泵(Beng)、进(Jin)样(Yang)器(Qi)、紫(Zi)外(Wai)检(Jian)测(Ce)器(Qi)、柱(Zhu)温(Wen)箱(Xiang)和(He)Empower色(Se)谱(Pu)工(Gong)作(Zuo)站(Zhan)组(Zu)成(Cheng)。5.1.2 电(Dian)源(Yuan):泵(Beng)为(Wei)220V稳(Wen)压(Ya)电(Dian)源(Yuan),检(Jian)测(Ce)器(Qi)为(Wei)220V稳(Wen)压(Ya)电(Dian)源(Yuan),工(Gong)作(Zuo)站(Zhan)为(Wei)220V稳(Wen)压(Ya)电(Dian)源(Yuan)。5.2 外(Wai)部(Bu)硬(Ying)件(Jian)的(De)操(Cao)作(Zuo):5.2.1依(Yi)次(Ci)打(Da)开(Kai)电(Dian)脑(Nao)、液(Ye)相(Xiang)分(Fen)离(Li)单(Dan)元(Yuan)和(He)检(Jian)测(Ce)器(Qi)电(Dian)源(Yuan),液(Ye)相(Xiang)分(Fen)离(Li)单(Dan)元(Yuan)进(Jin)行(Xing)开(Kai)机(Ji)自(Zi)检(Jian)(注(Zhu):打(Da)开(Kai)顺(Shun)序(Xu)错(Cuo)误(Wu)可(Ke)导(Dao)致(Zhi)软(Ruan)件(Jian)与(Yu)仪(Yi)器(Qi)连(Lian)接(Jie)不(Bu)上(Shang))。同(Tong)时(Shi)检(Jian)查(Cha)流(Liu)动(Dong)相(Xiang)和(He)10%甲(Jia)醇(Chun)的(De)体(Ti)积(Ji)是(Shi)否(Fou)充(Chong)足(Zu)。5.2.2开(Kai)机(Ji)自(Zi)检(Jian)后(Hou),"分(Fen)离(Li)单(Dan)元(Yuan)"将(Jiang)进(Jin)入(Ru)Idle(空(Kong)闲(Xian))模(Mo)式(Shi)。5.2.3冲(Chong)洗(Xi)密(Mi)封(Feng)垫(Dian),主(Zhu)屏(Ping)幕(Mu)下(Xia)按(An)【Diag】→"Diagnosities"界(Jie)面(Mian),按(An)Prime Seal Wash显(Xian)示(Shi)"Prime Seal Wash"屏(Ping)幕(Mu),按(An)【Start】,待(Dai)排(Pai)放(Fang)口(Kou)有(You)水(Shui)流(Liu)出(Chu)(气(Qi)泡(Pao)排(Pai)净(Jing))时(Shi)(约(Yue)1分(Fen)钟(Zhong)),按(An)【Halt】停(Ting)止(Zhi),按(An)【Close】关(Guan)闭(Bi)界(Jie)面(Mian)。(注(Zhu):10%甲(Jia)醇(Chun)足(Zu)够(Gou)多(Duo))5.2.4冲(Chong)洗(Xi)进(Jin)样(Yang)针(Zhen),按(An)Prime Ndl Wash 显(Xian)示(Shi)"Prime Ndl Wash"屏(Ping)幕(Mu),按(An)【Start】,待(Dai)自(Zi)动(Dong)停(Ting)止(Zhi)。清(Qing)洗(Xi)两(Liang)次(Ci),按(An)【Close】关(Guan)闭(Bi)界(Jie)面(Mian)。(注(Zhu):可(Ke)配(Pei)制(Zhi)与(Yu)实(Shi)验(Yan)用(Yong)流(Liu)动(Dong)相(Xiang)相(Xiang)同(Tong)溶(Rong)液(Ye))5.2.5湿(Shi)法(Fa)灌(Guan)注(Zhu):按(An)【Exit】退(Tui)出(Chu)"Diagnosities"界(Jie)面(Mian),按(An)【Menu/Status】,进(Jin)入(Ru)"Status(1)"屏(Ping)幕(Mu),在(Zai)"Compomtion"中(Zhong)对(Dui)所(Suo)灌(Guan)注(Zhu)的(De)管(Guan)路(Lu)输(Shu)入(Ru)100%,按(An)【Direct Function】,光(Guang)标(Biao)选(Xuan)"Wet Prime",按(An)【Enter】,显(Xian)示(Shi)"Wet Prime"后(Hou)按(An)【OK】,待(Dai)结(Jie)束(Shu)后(Hou),依(Yi)次(Ci)重(Zhong)复(Fu)操(Cao)作(Zuo)对(Dui)所(Suo)用(Yong)管(Guan)路(Lu)(A/B/C/D)进(Jin)行(Xing)灌(Guan)注(Zhu)。5.2.6冲(Chong)洗(Xi)自(Zi)动(Dong)进(Jin)样(Yang)器(Qi),在(Zai)"Status(1)"屏(Ping)幕(Mu)下(Xia),按(An)【Direct Function】,光(Guang)标(Biao)选(Xuan)"Purge Injector",按(An)【Enter】,显(Xian)示(Shi)"Purge Injector"界(Jie)面(Mian),按(An)【OK】。5.3点(Dian)开(Kai)Empower Pro软(Ruan)件(Jian)图(Tu)标(Biao),进(Jin)入(Ru)操(Cao)作(Zuo)界(Jie)面(Mian)。5.3.1 单(Dan)击(Ji)鼠(Shu)标(Biao)左(Zuo)键(Jian)进(Jin)入(Ru)"配(Pei)置(Zhi)系(Xi)统(Tong)"。选(Xuan)中(Zhong)"项(Xiang)目(Mu)"后(Hou),单(Dan)击(Ji) "新(Xin)建(Jian)项(Xiang)目(Mu)"。 出(Chu)现(Xian)"新(Xin)建(Jian)项(Xiang)目(Mu)向(Xiang)导(Dao)","表(Biao)空(Kong)间(Jian)"中(Zhong)接(Jie)受(Shou)50MB的(De)表(Biao)空(Kong)间(Jian)缺(Que)省(Sheng)设(She)置(Zhi)。在(Zai)该(Gai)向(Xiang)导(Dao)步(Bu)骤(Zhou)中(Zhong),系(Xi)统(Tong)默(Mo)认(Ren)设(She)置(Zhi)了(Liao)"支(Zhi)持(Chi)'全(Quan)面(Mian)审(Shen)计(Ji)追(Zhui)踪(Zong)'"。如(Ru)果(Guo)不(Bu)需(Xu)要(Yao),可(Ke)取(Qu)消(Xiao)"支(Zhi)持(Chi)'完(Wan)全(Quan)审(Shen)计(Ji)追(Zhui)踪(Zong)'"复(Fu)选(Xuan)框(Kuang),以(Yi)取(Qu)消(Xiao)对(Dui)项(Xiang)目(Mu)元(Yuan)素(Su)(如(Ru)方(Fang)法(Fa)和(He)样(Yang)品(Pin))所(Suo)做(Zuo)的(De)所(Suo)有(You)修(Xiu)改(Gai)的(De)记(Ji)录(Lu)。如(Ru)需(Xu)要(Yao),则(Ze)选(Xuan)中(Zhong)该(Gai)复(Fu)选(Xuan)框(Kuang)之(Zhi)后(Hou),还(Huan)再(Zai)选(Xuan)择(Ze)是(Shi)否(Fou)需(Xu)要(Yao)对(Dui)"方(Fang)法(Fa)变(Bian)化(Hua)"、"结(Jie)果(Guo)变(Bian)化(Hua)"、"样(Yang)品(Pin)信(Xin)息(Xi)变(Bian)化(Hua)"和(He)"删(Shan)除(Chu)"的(De)更(Geng)改(Gai)进(Jin)行(Xing)注(Zhu)释(Shi)。单(Dan)击(Ji)"下(Xia)一(Yi)步(Bu)"。"选(Xuan)项(Xiang)"页(Ye)中(Zhong),选(Xuan)择(Ze)用(Yong)于(Yu)本(Ben)项(Xiang)目(Mu)的(De)选(Xuan)项(Xiang)。单(Dan)击(Ji)"下(Xia)一(Yi)步(Bu)"。"访(Fang)问(Wen)控(Kong)制(Zhi)"页(Ye)中(Zhong),根(Gen)据(Ju)需(Xu)要(Yao)选(Xuan)择(Ze)设(She)置(Zhi)对(Dui)您(Nin)所(Suo)创(Chuang)建(Jian)的(De)项(Xiang)目(Mu)具(Ju)有(You)访(Fang)问(Wen)权(Quan)限(Xian)的(De)用(Yong)户(Hu)和(He)用(Yong)户(Hu)组(Zu)或(Huo)者(Zhe)接(Jie)受(Shou)缺(Que)省(Sheng)的(De)选(Xuan)项(Xiang),然(Ran)后(Hou)单(Dan)击(Ji)"下(Xia)一(Yi)步(Bu)"。 在(Zai)"复(Fu)制(Zhi)"中(Zhong),接(Jie)受(Shou)默(Mo)认(Ren)的(De)选(Xuan)项(Xiang),然(Ran)后(Hou)单(Dan)击(Ji)"下(Xia)一(Yi)步(Bu)"。在(Zai)"输(Shu)入(Ru)名(Ming)称(Cheng)"页(Ye)中(Zhong),输(Shu)入(Ru)项(Xiang)目(Mu)的(De)名(Ming)称(Cheng),必(Bi)要(Yao)时(Shi)输(Shu)入(Ru)注(Zhu)释(Shi)内(Nei)容(Rong)。最(Zui)后(Hou)单(Dan)击(Ji)"完(Wan)成(Cheng)"来(Lai)结(Jie)束(Shu)新(Xin)项(Xiang)目(Mu)的(De)创(Chuang)建(Jian)。 项(Xiang)目(Mu)列(Lie)表(Biao)中(Zhong)出(Chu)现(Xian)新(Xin)建(Jian)的(De)项(Xiang)目(Mu)名(Ming)称(Cheng)。5.3.2 分(Fen)析(Xi)方(Fang)法(Fa)的(De)建(Jian)立(Li):单(Dan)击(Ji)命(Ming)令(Ling)栏(Lan)上(Shang)的(De)View Method,如(Ru)果(Guo)出(Chu)现(Xian)"New Processing Parameters"页(Ye),选(Xuan)择(Ze) LC,然(Ran)后(Hou)单(Dan)击(Ji) OK。单(Dan)击(Ji)命(Ming)令(Ling)栏(Lan)上(Shang)的(De) Instrument Parameters。 仪(Yi)器(Qi)参(Can)数(Shu)出(Chu)现(Xian)在(Zai)"View Method"工(Gong)作(Zuo)区(Qu)中(Zhong),在(Zai)此(Ci)页(Ye)面(Mian)下(Xia),点(Dian)击(Ji)"Pump"设(She)置(Zhi):A泵(Beng)流(Liu)速(Su)、B泵(Beng)流(Liu)速(Su)、总(Zong)流(Liu)速(Su)以(Yi)及(Ji)柱(Zhu)温(Wen),柱(Zhu)压(Ya)上(Shang)限(Xian)一(Yi)般(Ban)设(She)在(Zai)3500,下(Xia)限(Xian)一(Yi)般(Ban)设(She)在(Zai)70。再(Zai)点(Dian)击(Ji)"UV Detector"设(She)置(Zhi):波(Bo)长(Chang)、单(Dan)双(Shuang)波(Bo)长(Chang)。 从(Cong)"File"菜(Cai)单(Dan)中(Zhong)选(Xuan)择(Ze) Save As。"Save current method"对(Dui)话(Hua)框(Kuang)将(Jiang)出(Chu)现(Xian),在(Zai)"Name"文(Wen)本(Ben)框(Kuang)中(Zhong)输(Shu)入(Ru)"方(Fang)法(Fa)名(Ming)称(Cheng)",在(Zai)"Comments"文(Wen)本(Ben)框(Kuang)中(Zhong)输(Shu)入(Ru)有(You)关(Guan)该(Gai)方(Fang)法(Fa)的(De)注(Zhu)释(Shi)(可(Ke)选(Xuan)),然(Ran)后(Hou)单(Dan)击(Ji)Save。5.3.3 平(Ping)衡(Heng)系(Xi)统(Tong):单(Dan)击(Ji)采(Cai)集(Ji)栏(Lan)上(Shang)的(De) (Equilibrate)。采(Cai)集(Ji)栏(Lan)上(Shang)"Status Information"部(Bu)分(Fen)将(Jiang)显(Xian)示(Shi)系(Xi)统(Tong)平(Ping)衡(Heng)的(De)状(Zhuang)态(Tai)。从(Cong)下(Xia)拉(La)列(Lie)表(Biao)中(Zhong)选(Xuan)择(Ze)"自(Zi)己(Ji)方(Fang)法(Fa)名(Ming)称(Cheng)",然(Ran)后(Hou)单(Dan)击(Ji) Equilibrate。为(Wei)系(Xi)统(Tong)留(Liu)出(Chu)大(Da)约(Yue)30分(Fen)钟(Zhong)以(Yi)上(Shang)时(Shi)间(Jian)进(Jin)行(Xing)平(Ping)衡(Heng),或(Huo)直(Zhi)到(Dao)基(Ji)线(Xian)稳(Wen)定(Ding)。5.4测(Ce)定(Ding)操(Cao)作(Zuo):5.4.1 单(Dan)针(Zhen)进(Jin)样(Yang),可(Ke)以(Yi)单(Dan)击(Ji)左(Zuo)下(Xia)角(Jiao)的(De)图(Tu)标(Biao),出(Chu)现(Xian)以(Yi)下(Xia)"单(Dan)针(Zhen)进(Jin)样(Yang)参(Can)数(Shu)"对(Dui)话(Hua)框(Kuang):在(Zai)Method 下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong),可(Ke)以(Yi)选(Xuan)择(Ze)指(Zhi)定(Ding)的(De)仪(Yi)器(Qi)参(Can)数(Shu),在(Zai)所(Suo)有(You)参(Can)数(Shu)设(She)定(Ding)完(Wan)毕(Bi)后(Hou),即(Ji)可(Ke)单(Dan)击(Ji)"Inject"键(Jian)开(Kai)始(Shi)进(Jin)样(Yang)。同(Tong)样(Yang)可(Ke)以(Yi)通(Tong)过(Guo)图(Tu)标(Biao)终(Zhong)止(Zhi)进(Jin)样(Yang)。5.4.2 样(Yang)品(Pin)组(Zu)进(Jin)样(Yang),a.在(Zai)"方(Fang)法(Fa)组(Zu)"下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong)选(Xuan)择(Ze)欲(Yu)使(Shi)用(Yong)的(De)方(Fang)法(Fa)组(Zu),同(Tong)时(Shi)在(Zai)下(Xia)方(Fang)的(De)"仪(Yi)器(Qi)方(Fang)法(Fa)"下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong),选(Xuan)择(Ze)欲(Yu)使(Shi)用(Yong)的(De)仪(Yi)器(Qi)方(Fang)法(Fa)。。b. 在(Zai)sample set 表(Biao)单(Dan)中(Zhong),逐(Zhu)行(Xing)填(Tian)写(Xie)"Sample Name"、"Function"以(Yi)及(Ji)"Method"与(Yu)"Run Time"、"Inj of Vail"" # of Injs"后(Hou),即(Ji)可(Ke)点(Dian)击(Ji)图(Tu)标(Biao)。c. 一(Yi)旦(Dan)点(Dian)击(Ji)图(Tu)标(Biao)后(Hou),会(Hui)出(Chu)现(Xian)如(Ru)下(Xia)"Run Sample Set"对(Dui)话(Hua)框(Kuang):在(Zai)对(Dui)话(Hua)框(Kuang)中(Zhong)写(Xie)入(Ru)样(Yang)品(Pin)组(Zu)的(De)名(Ming)称(Cheng),然(Ran)后(Hou)点(Dian)击(Ji)"Run",即(Ji)可(Ke)运(Yun)行(Xing)样(Yang)品(Pin)组(Zu)。d. 如(Ru)果(Guo)运(Yun)行(Xing)中(Zhong)需(Xu)要(Yao)终(Zhong)止(Zhi)样(Yang)品(Pin)组(Zu)的(De)运(Yun)行(Xing),可(Ke)点(Dian)击(Ji)图(Tu)标(Biao),终(Zhong)止(Zhi)运(Yun)行(Xing)。5.5 数(Shu)据(Ju)的(De)处(Chu)理(Li)5.5.1 利(Li)用(Yong)向(Xiang)导(Dao)建(Jian)立(Li)处(Chu)理(Li)参(Can)数(Shu)a.在(Zai)Find Data中(Zhong)的(De)选(Xuan)中(Zhong)要(Yao)处(Chu)理(Li)的(De)样(Yang)品(Pin),单(Dan)击(Ji)(Review,查(Cha)看(Kan))图(Tu)标(Biao),打(Da)开(Kai)数(Shu)据(Ju)。b. 单(Dan)击(Ji)(处(Chu)理(Li)方(Fang)法(Fa)向(Xiang)导(Dao),Processing Method Wizard),出(Chu)现(Xian)对(Dui)话(Hua)框(Kuang)。c. 选(Xuan)择(Ze)"Start New Processing Parameters" (建(Jian)立(Li)新(Xin)的(De)处(Chu)理(Li)参(Can)数(Shu))。然(Ran)后(Hou)单(Dan)击(Ji)"OK"。d. 如(Ru)果(Guo)出(Chu)现(Xian)下(Xia)面(Mian)的(De)对(Dui)话(Hua)框(Kuang),选(Xuan)择(Ze)"LC",然(Ran)后(Hou)单(Dan)击(Ji)OK。e. 在(Zai)"Integration-Integration Region"页(Ye)面(Mian)中(Zhong),在(Zai)空(Kong)格(Ge)中(Zhong)输(Shu)入(Ru),或(Huo)者(Zhe)在(Zai)图(Tu)上(Shang)用(Yong)鼠(Shu)标(Biao)左(Zuo)键(Jian)拖(Tuo)拽(Zhuai)来(Lai)选(Xuan)择(Ze)积(Ji)分(Fen)的(De)起(Qi)止(Zhi)时(Shi)间(Jian),然(Ran)后(Hou)单(Dan)击(Ji)"Next"。f. 出(Chu)现(Xian)"Peak Width and Threshold"页(Ye)面(Mian),接(Jie)受(Shou)默(Mo)认(Ren)的(De)数(Shu)值(Zhi),不(Bu)作(Zuo)改(Gai)动(Dong),单(Dan)击(Ji)"Next"。g. 在(Zai)"Peak Rejection"页(Ye)中(Zhong),根(Gen)据(Ju)需(Xu)要(Yao)设(She)定(Ding)最(Zui)小(Xiao)面(Mian)积(Ji)和(He)/或(Huo)者(Zhe)最(Zui)小(Xiao)峰(Feng)高(Gao)(也(Ye)可(Ke)不(Bu)设(She)),然(Ran)后(Hou)单(Dan)击(Ji)"Next"。h. 在(Zai)"Calibration-General"页(Ye)中(Zhong),选(Xuan)择(Ze)定(Ding)量(Liang)的(De)方(Fang)式(Shi):Area,校(Xiao)正(Zheng)曲(Qu)线(Xian)的(De)拟(Ni)合(He)方(Fang)式(Shi):Linear(线(Xian)性(Xing))。然(Ran)后(Hou)单(Dan)击(Ji)"Next"。i. 在(Zai)"Name" 栏(Lan)中(Zhong)编(Bian)辑(Ji)组(Zu)分(Fen)名(Ming)称(Cheng)(注(Zhu)意(Yi),此(Ci)处(Chu)的(De)名(Ming)称(Cheng)必(Bi)须(Xu)与(Yu)在(Zai)前(Qian)面(Mian)"Alter Sample"中(Zhong)所(Suo)输(Shu)入(Ru)的(De)名(Ming)称(Cheng)一(Yi)致(Zhi))。然(Ran)后(Hou)单(Dan)击(Ji)"Next"。j. 在(Zai)此(Ci)页(Ye)面(Mian)中(Zhong),不(Bu)作(Zuo)任(Ren)何(He)改(Gai)动(Dong),单(Dan)击(Ji)"Next"。k. 在(Zai)此(Ci)页(Ye)面(Mian)中(Zhong),选(Xuan)择(Ze)校(Xiao)正(Zheng)的(De)类(Lei)型(Xing)(type of Calibration),如(Ru)为(Wei)外(Wai)标(Biao)法(Fa),选(Xuan)"External Standard Calibration",单(Dan)一(Yi)内(Nei)标(Biao)法(Fa)(即(Ji)较(Jiao)为(Wei)常(Chang)用(Yong)的(De)内(Nei)标(Biao)法(Fa))选(Xuan)择(Ze)"Single Internal Standard",并(Bing)在(Zai)下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong)选(Xuan)择(Ze)内(Nei)标(Biao)峰(Feng),然(Ran)后(Hou)单(Dan)击(Ji)"Next"。j. 出(Chu)现(Xian)"Method Name"页(Ye),输(Shu)入(Ru)方(Fang)法(Fa)名(Ming)称(Cheng),必(Bi)要(Yao)时(Shi)输(Shu)入(Ru)注(Zhu)释(Shi)(Comments)。单(Dan)击(Ji)"Finish"完(Wan)成(Cheng)向(Xiang)导(Dao)。k. 单(Dan)击(Ji) (Save all)保(Bao)存(Cun)全(Quan)部(Bu)。5.5.2 定(Ding)量(Liang)计(Ji)算(Suan)a. 回(Hui)到(Dao)"Find Data"的(De)Channel选(Xuan)项(Xiang)卡(Ka)。用(Yong)鼠(Shu)标(Biao)选(Xuan)择(Ze)标(Biao)样(Yang)以(Yi)及(Ji)未(Wei)知(Zhi)样(Yang)品(Pin)(注(Zhu)意(Yi)一(Yi)定(Ding)要(Yao)先(Xian)选(Xuan)择(Ze)标(Biao)样(Yang),再(Zai)选(Xuan)择(Ze)未(Wei)知(Zhi)样(Yang)),然(Ran)后(Hou)单(Dan)击(Ji)右(You)键(Jian)出(Chu)现(Xian)快(Kuai)捷(Jie)菜(Cai)单(Dan),选(Xuan)择(Ze)Process。出(Chu)现(Xian)如(Ru)下(Xia)窗(Chuang)口(Kou):在(Zai)Peocess中(Zhong),选(Xuan)"Use specified method"(使(Shi)用(Yong)指(Zhi)定(Ding)的(De)方(Fang)法(Fa)),并(Bing)在(Zai)下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong)选(Xuan)择(Ze)刚(Gang)才(Cai)利(Li)用(Yong)向(Xiang)导(Dao)建(Jian)立(Li)的(De)方(Fang)法(Fa)。单(Dan)击(Ji)"OK"。b.到(Dao)"Results"(结(Jie)果(Guo))选(Xuan)项(Xiang)卡(Ka)中(Zhong),单(Dan)击(Ji)"Updata"键(Jian)更(Geng)新(Xin)结(Jie)果(Guo)。c. 选(Xuan)中(Zhong)欲(Yu)浏(Zuo)览(Lan)的(De)结(Jie)果(Guo),单(Dan)击(Ji)(Review,查(Cha)看(Kan)),出(Chu)现(Xian)查(Cha)看(Kan)主(Zhu)窗(Chuang)口(Kou),在(Zai)色(Se)谱(Pu)图(Tu)下(Xia)方(Fang)的(De)"Peak"表(Biao)中(Zhong),"Amount"栏(Lan)中(Zhong),即(Ji)可(Ke)看(Kan)到(Dao)定(Ding)量(Liang)的(De)结(Jie)果(Guo)。d. 单(Dan)击(Ji)工(Gong)作(Zuo)栏(Lan)中(Zhong)的(De)(Calibration Curve,校(Xiao)正(Zheng)曲(Qu)线(Xian)),打(Da)开(Kai)校(Xiao)正(Zheng)曲(Qu)线(Xian)窗(Chuang)口(Kou)。窗(Chuang)口(Kou)的(De)上(Shang)部(Bu)为(Wei)曲(Qu)线(Xian)的(De)方(Fang)程(Cheng)等(Deng)内(Nei)容(Rong)。可(Ke)通(Tong)过(Guo)下(Xia)拉(La)菜(Cai)单(Dan)查(Cha)看(Kan)不(Bu)同(Tong)组(Zu)分(Fen)的(De)相(Xiang)关(Guan)信(Xin)息(Xi)。5.5.3数(Shu)据(Ju)的(De)打(Da)印(Yin)1. 在(Zai)"Results"选(Xuan)项(Xiang)卡(Ka)中(Zhong)选(Xuan)择(Ze)欲(Yu)打(Da)印(Yin)的(De)结(Jie)果(Guo),单(Dan)击(Ji)(预(Yu)览(Lan)出(Chu)版(Ban))。出(Chu)现(Xian)"打(Da)开(Kai)报(Bao)告(Gao)方(Fang)法(Fa)"对(Dui)话(Hua)框(Kuang)。可(Ke)以(Yi)选(Xuan)择(Ze)选(Xuan)择(Ze)"Use a Report Method that was generated to appropriate for the selected data(使(Shi)用(Yong)对(Dui)选(Xuan)中(Zhong)的(De)数(Shu)据(Ju)适(Shi)用(Yong)的(De)报(Bao)告(Gao)方(Fang)法(Fa))",或(Huo)者(Zhe)在(Zai)"Use the following Report Method(使(Shi)用(Yong)以(Yi)下(Xia)的(De)报(Bao)告(Gao)方(Fang)法(Fa))"下(Xia)拉(La)菜(Cai)单(Dan)中(Zhong)选(Xuan)择(Ze)适(Shi)当(Dang)的(De)报(Bao)告(Gao)方(Fang)法(Fa)(例(Li)如(Ru)LC Calibration Report,LC校(Xiao)正(Zheng)曲(Qu)线(Xian)报(Bao)告(Gao)),然(Ran)后(Hou)单(Dan)击(Ji)"OK"。2. 预(Yu)览(Lan)无(Wu)误(Wu)后(Hou),可(Ke)单(Dan)击(Ji),进(Jin)行(Xing)打(Da)印(Yin)。5.6关(Guan)机(Ji)操(Cao)作(Zuo):5.6.1全(Quan)部(Bu)测(Ce)定(Ding)完(Wan)毕(Bi)后(Hou),按(An)规(Gui)定(Ding)用(Yong)适(Shi)当(Dang)溶(Rong)剂(Ji)冲(Chong)洗(Xi)泵(Beng)、进(Jin)样(Yang)阀(Fa)、色(Se)谱(Pu)柱(Zhu)和(He)检(Jian)测(Ce)器(Qi)。5.6.2关(Guan)闭(Bi)检(Jian)测(Ce)器(Qi)、泵(Beng)及(Ji)其(Qi)他(Ta)部(Bu)件(Jian)电(Dian)源(Yuan)并(Bing)拔(Ba)下(Xia)各(Ge)插(Cha)头(Tou),做(Zuo)好(Hao)使(Shi)用(Yong)登(Deng)记(Ji)。5.7维(Wei)护(Hu)与(Yu)保(Bao)养(Yang):5.7.1试(Shi)验(Yan)所(Suo)用(Yong)的(De)流(Liu)动(Dong)相(Xiang)应(Ying)经(Jing)过(Guo)0.45?m的(De)膜(Mo)过(Guo)滤(Lv),以(Yi)降(Jiang)低(Di)色(Se)谱(Pu)柱(Zhu)受(Shou)污(Wu)染(Ran)的(De)程(Cheng)度(Du),延(Yan)长(Chang)使(Shi)用(Yong)寿(Shou)命(Ming)。5.7.2试(Shi)验(Yan)前(Qian)先(Xian)打(Da)开(Kai)电(Dian)源(Yuan)稳(Wen)压(Ya)器(Qi),待(Dai)电(Dian)压(Ya)稳(Wen)定(Ding)后(Hou),方(Fang)可(Ke)打(Da)开(Kai)仪(Yi)器(Qi)开(Kai)关(Guan)。5.7.3色(Se)谱(Pu)柱(Zhu)最(Zui)高(Gao)工(Gong)作(Zuo)压(Ya)力(Li)一(Yi)般(Ban)不(Bu)能(Neng)超(Chao)过(Guo)3500。5.7.4检(Jian)测(Ce)器(Qi)的(De)光(Guang)源(Yuan)具(Ju)有(You)一(Yi)定(Ding)的(De)使(Shi)用(Yong)时(Shi)间(Jian),所(Suo)以(Yi)每(Mei)次(Ci)在(Zai)进(Jin)样(Yang)品(Pin)前(Qian)半(Ban)小(Xiao)时(Shi)左(Zuo)右(You)打(Da)开(Kai),试(Shi)验(Yan)结(Jie)束(Shu)后(Hou),应(Ying)先(Xian)关(Guan)闭(Bi)检(Jian)测(Ce)器(Qi)电(Dian)源(Yuan)。5.7.5最(Zui)后(Hou)一(Yi)次(Ci)进(Jin)样(Yang)完(Wan)成(Cheng)后(Hou),应(Ying)用(Yong)流(Liu)动(Dong)相(Xiang)冲(Chong)洗(Xi)一(Yi)段(Duan)时(Shi)间(Jian),以(Yi)保(Bao)证(Zheng)洗(Xi)脱(Tuo)完(Wan)全(Quan),然(Ran)后(Hou)用(Yong)纯(Chun)水(Shui)冲(Chong)洗(Xi)约(Yue)半(Ban)小(Xiao)时(Shi),以(Yi)除(Chu)去(Qu)流(Liu)动(Dong)相(Xiang)中(Zhong)的(De)无(Wu)机(Ji)盐(Yan)类(Lei)。5.7.6最(Zui)后(Hou)用(Yong)甲(Jia)醇(Chun)对(Dui)色(Se)谱(Pu)柱(Zhu)进(Jin)行(Xing)再(Zai)生(Sheng)保(Bao)存(Cun)。5.7.7操(Cao)作(Zuo)者(Zhe)应(Ying)细(Xi)心(Xin)了(Liao)解(Jie)仪(Yi)器(Qi)各(Ge)部(Bu)件(Jian)性(Xing)能(Neng)。5.7.8每(Mei)次(Ci)操(Cao)作(Zuo)完(Wan)毕(Bi)后(Hou),应(Ying)及(Ji)时(Shi)清(Qing)理(Li)所(Suo)用(Yong)物(Wu)件(Jian),倒(Dao)掉(Diao)废(Fei)瓶(Ping)中(Zhong)的(De)废(Fei)液(Ye),用(Yong)柔(Rou)软(Ruan)的(De)抹(Mo)布(Bu)擦(Ba)拭(Shi)仪(Yi)器(Qi)表(Biao)面(Mian),保(Bao)持(Chi)仪(Yi)器(Qi)的(De)清(Qing)洁(Jie)。5.7.9若(Ruo)仪(Yi)器(Qi)长(Chang)时(Shi)间(Jian)不(Bu)用(Yong),可(Ke)定(Ding)期(Qi)加(Jia)电(Dian),使(Shi)仪(Yi)器(Qi)预(Yu)热(Re)一(Yi)段(Duan)时(Shi)间(Jian),以(Yi)免(Mian)仪(Yi)器(Qi)内(Nei)部(Bu)件(Jian)受(Shou)潮(Chao)。5.7.10为(Wei)保(Bao)证(Zheng)检(Jian)验(Yan)数(Shu)据(Ju)的(De)可(Ke)靠(Kao),每(Mei)年(Nian)应(Ying)由(You)计(Ji)量(Liang)部(Bu)门(Men)负(Fu)责(Ze)校(Xiao)验(Yan)一(Yi)次(Ci)。5.8数(Shu)据(Ju)安(An)全(Quan)与(Yu)备(Bei)份(Fen)管(Guan)理(Li)5.8.1 实(Shi)验(Yan)员(Yuan)使(Shi)用(Yong)前(Qian),首(Shou)先(Xian)必(Bi)须(Xu)分(Fen)别(Bie)授(Shou)权(Quan)软(Ruan)件(Jian)的(De)使(Shi)用(Yong)账(Zhang)号(Hao)和(He)密(Mi)码(Ma),并(Bing)且(Qie)确(Que)保(Bao)防(Fang)止(Zhi)泄(Xie)露(Lu)。不(Bu)同(Tong)实(Shi)验(Yan)员(Yuan)对(Dui)应(Ying)不(Bu)同(Tong)账(Zhang)号(Hao),不(Bu)得(De)共(Gong)享(Xiang)。5.8.2 未(Wei)经(Jing)质(Zhi)保(Bao)部(Bu)经(Jing)理(Li)允(Yun)许(Xu),任(Ren)何(He)人(Ren)不(Bu)得(De)私(Si)自(Zi)修(Xiu)改(Gai)仪(Yi)器(Qi)参(Can)数(Shu)、方(Fang)法(Fa)参(Can)数(Shu)。5.8.3 每(Mei)3个(Ge)月(Yue)对(Dui)各(Ge)账(Zhang)号(Hao)的(De)实(Shi)验(Yan)数(Shu)据(Ju)进(Jin)行(Xing)一(Yi)次(Ci)备(Bei)份(Fen),存(Cun)档(Dang)至(Zhi)其(Qi)他(Ta)受(Shou)控(Kong)的(De)计(Ji)算(Suan)机(Ji)中(Zhong)。

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